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BL04B1 OUTLINE

問い合わせ番号

INS-0000000317

ABSTRACT

  The BL04B1, “High Pressure and High Temperature” is a white X-ray beamline from a bending magnet. The use of high energy (20 - 150 keV) is suitable for energy-dispersive diffraction experiment using a solid state detector (SSD) and X-ray radiography experiment using a CCD camera. Moreover, the double silicon crystal monochromator can select the X-ray energy between 30 and 60 keV from synchrotron X-ray radiation through bending magnet, the 2D-XRD data is acquirable using imaging plate (IP) or large area CCD camera. This beamline is designed to conduct research on the structure and properties of materials in the Earth's interior under high-pressure and high-temperature conditions. High-pressure and high-temperature experiments are performed using two large-volume presses: SPEED-1500 and SPEED-Mk.II, both of which are installed in the tandem experimental stations (Experimental hutch 1, hutch 2) (Fig. 1). These large-volume presses are constructed by double-stage (Kawai-type) high-pressure vessels with two kinds of the anvils; the tungsten carbide (WC) and the sintered diamond (SD) (Fig. 2). 30 GPa or 100 GPa has been reached with the WC (26 × 26 × 26 mm3) or the SD (14 × 14 × 14 mm3) over 3000 K (Fig. 3), and its high pressure and high temperature condition is corresponding to the upper or the lower mantle region in Earth's interior.

AREA OF RESEARCH

  • X-ray diffraction measurements and radiography under extreme conditions using large-volume press up to 100 GPa/3000 K
  • Energy dispersive X-ray diffraction measurements (2θ = 3-20°/ 20-150 keV)
  • Angle dispersive X-ray diffraction measurements (30-60 keV/ 2θ = <10°)

KEYWORDS

  • Scientific field
    High-pressure, Geophysics.
  • Equipment
    Large-volume press, Energy-dispersive X-ray diffraction, Angle-dispersive X-ray diffraction, X-ray radiography

SOURCE AND OPTICS

BL04B1_opt1s.jpgBL04B1_opt2.jpgFig. 1. Layout of BL04B1 beamline.
1e.jpg

Fig. 2. The second stage anvils of the tungsten carbide (WC) and the sintered diamond (SD) cubes.

1companvil.jpg

Fig. 3. Comparisons of the pressure generations using the WC and the SD anvils.

    • X-rays at Sample

      Energy range 20 ∼ 150 keV (white)
      Beam size 0.05 × 0.05 ∼ 10 × 10mm2
      Beam divergence (V) < 0.05 mrad
      Beam divergence (H) < 0.5 mrad

EXPERIMENTAL STATIONS

PUBLICATION SEARCH

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BL04B1 PUBLICATION SEARCH

 

CONTACT INFORMATION

Please note that each e-mail address is followed by "@spring8.or.jp."

Yuji HIGO
SPring-8 / JASRI
1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198
Phone : +81-(0)791-58-2750
Fax : +81-(0)791-58-0830
e-mail : higo

Yoshinori TANGE
SPring-8 / JASRI
1-1-1 Kouto, Sayo-cho, Sayo-gun, Hyogo 679-5198
Phone : +81-(0)791-58-2750
Fax : +81-(0)791-58-0830
e-mail : yoshinori.tange

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